By A. N. Paruta, R. Piekos
One among 3 volumes which jointly hide all pronounced solubility info for an incredible pharmaceutical category: the sulfonamides. an information of solubility information is helpful in all pharmaceutical learn. released solubility facts for the identify compounds were compiled and severely evaluated, leading to steered solubility values which working towards scientists might use with self assurance. each one quantity contains structural formulae and molecular weight information for the compounds coated, comfortably grouped jointly
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Extra info for 4–Aminobenzenesulfonamides. 6-Membered Heterocyclic Substituents and Miscellaneous Systems
128, 537. Wochenschr. 29 COMPONENTS : (1) ORIGINAL MEASUREMENTS: Benzenesulfonamide, 4-amino-N-2- Neish, W. pyridinyl- 1948, C H N 11 11 3°2 (2) Water; (sulfapyridine); S; H 20 ; J. 67, Reo. P. trav. ohim. 361-71. [144-83-2] [7732-18-5] VARIABLES : PREPARED BY: One temperature: 37°C R. 48 χ 1 0 ~ mol dm 3 , compiler ) . AUXILIARY INFORMATION METHOD/APPARATUS/PROCEDURE : A suspension of sulfapyridine SOURCE AND PURITY OF MATERIALS: (10 mg/5 ml) in water was kept for 5 h at 37°C and 1 h at room temp before fitration.
18 COMPONENTS : (1) ORIGINAL MEASUREMENTS: Benzenesulfonamide, 4-amino-N-[4- Gutierrez, [(dimethylamino)sulfonyl]phenyl]-; C1 H 4 1 N 7 30 4S 2; (2) 2-Propanone Anales [515-67-3] (acetone); F. H. Fis. quim. (Madrid) 41, 1945, 537-60. C^H^O; [67-64-1] VARIABLES : PREPARED BY: Temperature EXPERIMENTAL VALUES: t/°C G a E R. 57 10 28 036 21 897 225 129 633 45 8 3 56 4 44 15 29 064 22 519 231 669 654 47 5 3 44 4 31 20 30 092 23 130 238 072 672 49 0 3 32 4 20 25 31 120 23 733 244 354 689 50 9 3 21 4 09 30 31 898 24.
Thermostat. Purity of the water was not specified. The equilibrium was usually at- tained after 1 h. Five to 100-cm Its samples of the satd soin were placed in Pt crucibles or dishes and evapd to dryness at temps lower than 110-115°C. The residue was dried to const wt at 105-110°C and weighed. E S T I M A T E D E R R O R : Soly: quite reliable results were obtained over the temp range 20-75°C. At higher temps the accuracy was poor due to evapn of water during sampling (authors). 05°C (authors).
4–Aminobenzenesulfonamides. 6-Membered Heterocyclic Substituents and Miscellaneous Systems by A. N. Paruta, R. Piekos